Author Archives: chemweb

HMQC, HSQC and HMBC experiments now work well on the I500 after an unstable broadband RF amplifier was replaced. We have optimized two HSQC experiments for the I500: “iuhsqc” gives higher sensitivity, “iuhsqcad” gives better quality (less artifacts). Continue reading →

All the spectrometers are operational after the power outage this morning. Continue reading →

HMQC, HSQC and HMBC experiments currently are not working well on the I500 due to a hardware problem. All other experiments, including routine 1H, 13C, COSY, NOESY, ROESY, etc. work with no problem. Continue reading →

No lab gloves are allowed in the NMR facility. Only capped or sealed tubes are allowed in the NMR facility. All other chemistry (titrations, etc.) must be done elsewhere. A small wet lab (237A) is available off the NMR facility … Continue reading →

Both 600 and 800 spectrometers are operational. Continue reading →

You might have encountered some difficulties with Autolock on the I400 and I500 due to a Lockphase change after the last week’s power outage. This problem has been fixed. Continue reading →

After the power outage today. Continue reading →

Chemistry NMR will be available 24/7 as usual and will be unstaffed Mon. 12/26, Thurs. 12/29 and Fri. 12/30. Continue reading →

The old Lexmark printer for the i400 has been replaced by a new HP Laserjet printer. The old printer is now installed on the i500 for light-duty jobs. Continue reading →

The Chemistry NMR lab was getting warm on Saturday due to a problem on the building temp control system for this area. The room temperature has been back to normal today. All spectrometers are operational. Continue reading →