Category Archives: Uncategorized
HMQC/HSQC/HMBC not work on I500
HMQC, HSQC and HMBC experiments currently are not working well on the I500 due to a hardware problem. All other experiments, including routine 1H, 13C, COSY, NOESY, ROESY, etc. work with no problem. Continue reading
Safety Reminder
No lab gloves are allowed in the NMR facility. Only capped or sealed tubes are allowed in the NMR facility. All other chemistry (titrations, etc.) must be done elsewhere. A small wet lab (237A) is available off the NMR facility … Continue reading
600 is back up
Both 600 and 800 spectrometers are operational. Continue reading
I400 & I500 Autolock Problem Fixed
You might have encountered some difficulties with Autolock on the I400 and I500 due to a Lockphase change after the last week’s power outage. This problem has been fixed. Continue reading
Chemistry NMR is back up!
After the power outage today. Continue reading
NMR holiday hours
Chemistry NMR will be available 24/7 as usual and will be unstaffed Mon. 12/26, Thurs. 12/29 and Fri. 12/30. Continue reading
I400 has a new printer, i500 gets the used one
The old Lexmark printer for the i400 has been replaced by a new HP Laserjet printer. The old printer is now installed on the i500 for light-duty jobs. Continue reading
Room temperature back to normal
The Chemistry NMR lab was getting warm on Saturday due to a problem on the building temp control system for this area. The room temperature has been back to normal today. All spectrometers are operational. Continue reading
600 cold probe down
Due to the malfunctioning compressor for the 600 cold probe, 600 is not operational. Continue reading
Unstaffed November 24th & 25th
Both the Chemistry and Simon NMR facilities will be unstaffed on November 24th & 25th. Continue reading