How to set up expt. on Bruker Avance Neo 600

1. ej and ij to eject or insert your nmr sample with holder.

2. edte to change the temperature you want:

3. new to open a dataset you want:

4. lock to lock to the right solvent:

5. atma to automatically do tuning and matching:

6. topshim 1d ordmax=8 ss

topshim tune tunea

7. getprosol to read in the parameters from probe file.

8. pulsecal to calibrate 1H 90:

9. O1cal to get o1 value:

10. eda to update other parameters: ns, sw, sw1, sw2, o2, o3, check “ –DLABEL_CN” option:

11. rga to get right rg

12. zg to start the current expt.

13. rser 1


to check how the first fid looks like.

edited on 6/11/18, by HW

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