How to process NUS 2D spectra collected from B600:

  1. For 2D spectra, set NusAmount from 25% to 50% (~40% is good).
  2. Use bruker –nus to create fid.com macro, (update the referencing parameters with the right values by your pp macro), and it outputs two files: test.fid and mask.fid.
  3. Run fid_2d.com macro, and it outputs test.ft2, and use for phase correction and indirect dimension reversion if needed, (and nmr.com macro will be created too).
  4. Run fid_nus2d.com macro to output final  2D spectra.

fid_2d.com:

#!/bin/csh

basicFT2.com -in test.fid -out test.ft2 \

-xP0  208 -xP1 0 -xEXTX1 9.5ppm -xEXTXN 6.0ppm \

#       -yFTARG alt,neg \

-yP0 82 -yP1 0 \

—————————————————————

fid_nus2d.com:

#!/bin/csh

ist2D.com \

-in test.fid -mask mask.fid -out test_2dnus.ft2 \

-xP0  208 -xP1 0 -xEXTX1 9.5ppm -xEXTXN 6.0ppm \

#       -yFTARG alt,neg \

-yP0 82 -yP1 0 \

 

Hongwei updated on 9/16/2021

Edited on 6/11/2018

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